METS

Metallurgical Testwork Print


Metallurgical Testplan

Comminution Tests

Benchscale Tests

Variability Testwork

Pilot Testing

 

Metallurgical Testplan


The development of a suitable process to treat an orebody appears to be a relatively straightforward matter. However, selecting the optimum process whilst maintaining the overall project development schedule is a complex task. This requires careful balancing of time and budgetary constraints against the benefits of a more closely defined process design.The key to a successful process plant design is the implementation of a well-structured, comprehensive testwork program to ensure that a circuit and reagent scheme is developed that can cater for the variability in the orebody, whilst still providing near optimum economics on the majority of the process plant feed.It is important that Metallurgical Testplan is developed and executed in parallel with the exploration of the deposit and that the results are used to assist in the planning and understanding of the continuing exploration. An understanding of the geology and mineralogy of a deposit, and the consequent sample selection for testwork, has a significant impact on the effectiveness of the plant design. The following factors are important in ensuring that an integrated approach to the design of the processing plant is achieved:

  • Understanding the deposit from a process perspective by the geology and mining disciplines;
  • Detailed evaluation of geology, mineralogy and mining method of the deposit by the process design team; and
  • Assessment of the metallurgical requirements for sample selection.

Frequently, there is insufficient interaction between the major disciplines and this can adversely affect the costs and schedule of the process design phase and, ultimately, the commissioning and operation of the project. The basic mineralogy and geology of a deposit dictate the plant design and testwork requirements and it is important that the whole team has an appreciation of the extractive metallurgy of the ore. For this to occur, process input is required early in the exploration phase to ensure that potential process issues are addressed. For example, exploration drilling and geological analysis can infer a potentially economic gold deposit based solely on gold grades. However, process factors, such as refractoriness leading to low recovery or gangue components leading to high reagent consumption, can complicate the processing of the ore and may render the deposit uneconomic.It is necessary that such issues are identified and understood so that process variables can be assessed throughout the evaluation phase. Metallurgical testwork can be used to evaluate process options that, in turn, can significantly impact on the exploration and geological requirements.It is also important that the exploration and mining teams have an understanding of the potential process implications of the ore. It is not uncommon that a deposit is almost completely explored and a mine plan developed without qualified process input. This can create a disjointed approach to the development of the project. The mine plan can be completely in disagreement with the optimum processing requirements. Either the process design has to be modified to suit the mine plan or a new iteration of the mining plan is required to better suit the processing requirements. Either way, both money and time can be wasted. The optimum mine plan must recognise the balance between low cost, bulk, non-selective mining and the requirements of the process plant in treating the different ore types within the orebody.Before designing a sample collection and testwork program, a thorough understanding of the ore types to be processed is necessary. The process design team must be able to categorise the deposit into areas possibly requiring different processing methods. Therefore, the first stage in the process design must be a complete review of the geology and mineralogy of the deposit. In parallel with this, the mining methods and mine plans should also be assessed. Whilst the results of testwork programs can be used to differentiate between ore types, the cost and time requirements for testwork programs can be reduced significantly through prior use of geological and mineralogical data.

Factors that should be considered in the sampling and testwork program include:

  • General Ore Type: The general type of ore will ultimately dictate the plant design and the detail of sampling and testwork required. A simple, near-surface, free-milling gold ore may require only a small amount of sampling and testwork. A complex base metals sulphide deposit will dictate a much more detailed sampling and testwork program due to the increased technical complexity and risk associated with the plant design.
  • Multiple Deposits: It is common that ores from multiple deposits or pits will be treated in one processing plant. These deposits may vary significantly and may impact on the whole methodology of the project development. It is also important to understand the metallurgical variability within each of these deposits, regardless of how small they may be. As a general rule of thumb, individual Metallurgical Testwork should be carried out on each pit which represents more than 10% of whole ore deposit.
  • Different Ore Lodes or Lenses: Within a single deposit, there can be significant changes in ore characteristics between different lodes or lenses.
  • Rock Type Variations: There may be significant variations in rock types, both in the ore and in host rock that should be considered.
  • Depth: Mineralogy often changes with depth. The process plant typically receives ore from different depths, in accordance with the mine plan, especially from open pits. Hence, depth is a variable to be accounted for in the design of a sampling program. Oxidation of the upper areas of a deposit commonly leads to the formation of oxide and transitional ore zones above the primary ore zones. Each zone can respond differently to a metallurgical process, and a staged approach to processing may be required with different processing strategies for each ore zone. So each zone needs a separate Metallurgical Testplan.
  • Head Grade: Head grade of valuable metal is often the only quantitative datum available across the deposit. Therefore, sample collection and testwork should recognise head grade as an important variable. It is important that head grade analysis is not confined to the valuable elements, but also includes those elements which can constrain throughput and recovery, eg. sulfur and arsenic values in a gold deposit. Failure to recognise this has been noticeable in some refractory gold projects. It is a significant omission, since the throughput of the oxidation circuits is dictated by sulfur grade.

 

metallurgical

Mining Plan: The mining plan dictates a schedule of ore delivery to the process plant. The ore characteristics can significantly change over the life of the mine and may influence the plant design. The requirement for campaign processing or blending of ore types should be considered in Metallurgical Testwork.

Sample Selection for Metallurgical Testwork

The aim of a sampling program is to collect the optimum number and quantity of samples that allows a suitable plant to be designed and metallurgical performance to be predicted.

For a completely homogenous orebody, a single sample could be used. However, no deposit is this simple and, typically, there are variations of rock type, ore grade and mineral occurrence with which to contend. A single representative sample, composited from a weighted average of all ore types, is unlikely to be suitable for evaluation of plant design and metallurgical recovery and grade. This is because ore is seldom presented to the processing plant in such a manner.

Unless a significant blending process is allowed for prior to processing, varying ore types can be mined and processed with little or no blending. The design of the plant, therefore, has to cater for the anticipated schedule of ore for treatment and sample collection for a Metallurgical Testplan must recognise this.

Typically, three major sample types are used in the metallurgical evaluation of a deposit:

  • Variability Samples: These are individual drill hole intersections or specific composites that represent ore types exhibiting different metallurgical responses, as indicated by the mineralogy/geology and expected process performance. They are used to assess the variability of the orebody, to determine whether the plant design will be suitable for all ore types, and to evaluate metallurgical recovery and/or grade. In this context, it is also important to ensure that testwork is carried out on samples representing the ore to be fed initially to the plant.
  • Composite Samples: Composite samples are used for testing reagent or flowsheet variables where comparative testwork must be carried out on the one sample. Typically, several composite samples may be required to assess the major ore types. The number of these composites needs to be rationalised to minimise testwork costs and time.

The composites should represent the ore types that will dictate the plant design, eg. The hardest major ore type, the most difficult ore to float, etc. Factors that should be considered in sample composition and representivity include:

  • metallurgical and geological definition of the "ore type"
  • variability of the ore (continuity of mineralisation)
  • the number of intersections included in the composite
  • the drill hole intersection angles through the orebody
  • special distribution of intersections
  • weighting of intersection samples to make up the composite

There is little value in trying to achieve a representative composite of the entire deposit, as the processing plant will probably never treat such ore at any one time.

  • Bulk Samples: Bulk samples are used for pilot plant testing or large scale tests. Pilot plant tests are usually required to demonstrate a high risk process, to increase the confidence level on a marginal project or for the production of concentrate or other downstream products for other testwork (eg. roasting). Pilot plant testwork does not necessarily provide better testwork data than bench scale work and should be evaluated carefully in terms of the high cost of sample collection and the difficulty in achieving adequate sample representation.

Types of Sample for Metallurgical Testwork

There are several types of sample material commonly used for metallurgical testwork:

Reverse Circulation (RC) Drill Chips - Fundamental problems caused by the stratification of heavy particles within RC drill chip samples can result in poor representation. The RC chips also tend to have a bimodal size distribution, with both coarse chips and a large amount of very fine material. The problem is exacerbated with friable ore types, eg. sericites, and can affect testwork results. This leads to another problem arising from the potential oxidation of the sample due to the high fines content. Despite the problems with RC drill chips, the low cost of sample collection compared with other methods makes it a popular choice for simple metallurgical tests such as gold and copper leaching tests. Their use in comminution and flotation tests should, generally, be avoided.

 

RC

 

Diamond Drill Core - Fresh diamond drill core provides excellent material for metallurgical testwork. Comminution and flotation testwork generally requires drill core of varying sizes to achieve satisfactory results. NQ (50 mm) and HQ (63 mm) diamond drill core is commonly available from the exploration phase. The core is usually cut into quarters. Typically, only one quarter will be available for metallurgical testwork. There is a number of comminution tests that require at least whole (uncut) HQ core or whole PQ (75 mm) core. Drilling program plans should account for these process sample requirements and may need to include holes drilled specifically for metallurgical sample collection.

DIAMONDDRILLCORE

Trial Mine Samples - Large samples can be generated from RC chips or drill core, but, as the quantity requirements increase, trial open cut or underground mining may become more economic. Unfortunately, costs usually impose significant limitations with mined bulk samples.

Testwork Required for Engineering Studies

There are different types of the tests which will be carried out based on the type and level of the studies as shown in Table next page. The cost associated with each level of these studies is estimated as follows:

  • Conceptual Study- $50,000 +/-20%
  • Pre feasibility Study- $200,000 +/- 50% (Simple gold ore, one orebody)
  • Bankable Feasibility Study- $500,000 +/- 50% (Simple gold ore)
  • Bankable Feasibility Study- $1,000,000 (Base metals + Pilot Plant)
FEASIBLITITY STUDIES

 


Comminution Tests


 

The term comminution in a mineral processing plant or mill refers to the sequence of crushing and grinding. Comminution circuits invariably account for a major portion of the capital and operating costs of the process plant. Therefore, the design and engineering of this unit operation, play a major role in maximising the net present value of the project. Decision-making in this area has, as one of its key objectives, the need to balance operating phase risks against capital costs.A number of flowsheet options exist for the comminution of an ore. The flowsheet selection and/or optimisation is based on the characterisation of the ore. The ore characterisation can be ascertained by the following tests:

 

  1. Bond Rod Mill Work Index (RWI)
  2. Bond Ball Mill Work Index (BWI)
  3. Abrasion Index Test (AI)
  4. Crushing Work Index (CWI)
  5. JK Drop Weight Test
  6. Point Load Test (PLT)
  7. SAG Mill Comminution (SMC) Test
  8. Unconfined Compression Strength (UCS) Test

Bond Rod Mill Work Index (RWI)

RWI
The Bond Rod Mill Work Index (RWI) is a value that gives a measure of the energy needed to grind an ore sample from 12.5 mm as feed to a rod mill, to  about 1mm. The RWI derived is used for determining (with other factors) whether critical size will form in a SAG mill. The RWI can define the ore as:
  • Soft (7-9 kWh/t)
  • Medium (9-14 kWh/t)
  • Hard (14-20 kWh/t)
  • Very hard (>20 kWh/t) 
To interpret the result RWI, the higher the RWI value, then the larger the amount of energy that is required and therefore a larger mill. A minimum of 15 kg of material (usually drill core) crushed to a nominal size of -12.5 mm is required. The test is conducted  to achieve a stable 100% circulating load.

Bond Ball Mill Work Index (BWI)

BWI

The Bond Ball Work Index (BWI) is an indication of how much energy is required to grind a sample in a ball mill, from 3.35mm to about 0.075mm. The BWI can categorise the sample as:

  • Soft (7-9 kWh/t)
  • Medium (9-14 kWh/t)
  • Hard (14-20 kWh/t)
  • Very hard (>20 kWh/t)
Based on the BWI and utilising other parameters, it is then possible to calculate the design size of the mill based on ore throughput. A standard test would require a minimum of 10 kg of material crushed to a nominal size of -3.35 mm. (core is preferred)

 

Abrasion Index Test (AI)

AI
The Abrasion Index (AI) provides an indication of the metal wear rates in crushers, (such as liner wear rates), and grinding media consumption rates, (i.e. ball charge loads for ball mills). Such wear indications are needed to give accurate operating cost estimates. The result of the AI test indicates the amount of wear experienced by a plate in a standard wear test. It is an Index and typical mining industry values are about 0.3, with a high value being 0.8. . Each ore type that will be processed in the plant should be tested.Sample requirements for this test will need 1.6 kg of -19.7+12.5 mm of representative crushed ore.

Crushing Work Index (CWI)

The Crushability Test gives a guide to the impact resistance of the ore. A succession of rocks are broken by a calibrated hammer and the energy per unit mass for breakage developed. This is expressed as the Crushing Work Index (CWI). The test can be performed on core, cubed or cylindrical, or natural size samples. The CWI can therefore determine the crushability based on units of kWh/t. CWI used for calculating crusher power requirements and describes the competency of an ore at larger particle sizes. Values of Bond crushing work index will vary from a 8 kWh/t for laterite hardcap through to 22 kWh/t for banded iron formation to 46 kWh/t for fresh greenstone.Twenty rock specimens sized at -76+51 mm are needed for testing. The suggested core types are PQ core or large lump ore.

JK Drop Weight Test

The aim of the JK Drop Weight Test is to determine rock breakage parameters, A and b, that are used to analyse and predict autogenous (AG) and semi-autogenous (SAG) mill performance. Different energy inputs are tested on the ore at different fraction ranges of 13 to 63 mm on the ore. The results of the test are collated and the parameters, A and b are determined.  The parameters are used in a modelling simulation package (JKSimMet simulator software), which can determine the energy requirement of a grinding circuit and simulate a mill to handle many different breakage sizes. It is then possible to simulate the operation of the circuit in situations when there is a change in feed size distribution, ball load, etc. This simulation provides the sizing data for SAG Milling. The BWI suite is also needed for this simulation. To carry out this test, a minimum of 65 kg of whole core samples (full PQ core) is required. Each ore type that will be processed in the plant should be tested.
JK DROP WEIGHT
Property Very hard Hard Mod. Hard Medium Mod Soft Soft Very Soft
A*b <30 30-38 38-43 43-56 56-67 67-127 >127
ta <0.24 0.24-.035 0.35-0.41 0.41-0.54 0.54-0.65 0.65-1.38 >1.38

 

JK Simulation

 JK simulation allows laboratory data to be modelled as a circuit and various parameters to be changed or different circuit configurations used. This minimises the process risk and allows optimisation of the circuit. JK SIM

Point Load Test (PLT)

The objective of the Point Load Test (PLT) is to determine the ‘Uncorrected Point Load Strength Index’, Is. The index is corrected to the index value to a standard equivalent of a 50 mm core to yield a IS (50) value. This corrected value characterises the rock strength properties of the sample, such as uniaxial, tensile and compressive strength. This test is similar to UCS but is more cost effective.

To determine Point Load Index, a minimum of 10 core samples is required where the length to diameter ratio of sample is more than 2.5:1 and an ideal diameter of 50 mm. Irregular pieces of rock that are 20-60 mm in diameter with the same aspect ratio of 2.5:1 are also acceptable for testing. Each ore type should be tested.

PLT

 

SAG Mill Comminution (SMC) Test

The Sag Mill Comminution (SMC) Test is a lower cost version of the JK Drop Weight Test which tests on small rocks or quarter split drill cores. The test is performed on a single size fraction to determine the A and b parameters which are used in JKSimMet simulations to model the behaviour of a circuit mill for troubleshooting purposes, process change, design equipment size, etc. For the SMC test, a minimum of 60 rocks or quarter split core PQ core size. For testing of an ore a minimum of 10 kg is required.
SAG MILL

 

Unconfined Compression Strength (UCS) Test

The Unconfined Compressive Strength (UCS) Test indicates the shear strength by applying compression to the sample until it fails. It is vital for crusher selection and in assessing the suitability of an ore for milling. Drill core can be used for testing. Each ore type that will be processed in the plant should be tested.In this test, drill core samples of length to diameter ratio of more than 2:1 are required.
UCS

 

Mpa

50-100                         soft oxide ores              high crushing rates

101-250                       medium hard              average crushing rates

251-400                       hard ore                       reduced throughput

400>                            very hard ore                crushing difficult, high power

 

Ultra Fine Grinding 
The IsaMill is a horizontal high speed stirred mill that operates with high power intensities and uses fine, inert media such as river sand, smelter slag or ceramic beads. The mill is shown schematically in the Figure below.    

isamill_schematic.jpg 

  IsaMill Schematic 

With high power efficiency and grinding to less than 12 microns, the IsaMill technology quickly became very reliable. MIM's development uses relatively cheap materials like rubber and polyurethane compounds that offer long wear lives.  

The grinding chamber consists of a horizontally mounted shell and has a volume of approximately 3000 litres. A shaft is coupled to a motor gearbox driven by a 1500 kW motor where rotating grinding discs are mounted onto the shaft system.  Media and ore particles are continuously fed into the feed ports and mixed in a slurry. A product separator separates the exiting fine product and the media remains inside the mill.       

Some common applications in gold recovery include fine grinding of sulfide concentrates for the conventional cyanide leaching of gold. There is also fine grinding of sulfide concentrates for oxidative leaching processes for production of copper or nickel metal.

 

Benefits of IsaMill

·          Low maintenance - simple operation requires few specialists.

·          Compact - the mill system is the smallest of fine grinding equipment.

·          High Energy intensity - high power efficiency with up to 1.1MW operation.

·          Accurate scale-up - good accuracy from pilot to commercial sizes.

 

 Signature plots can be prepared on samples in a test mill.


 

Benchscale Tests


Benchscale Tests includes the following :

  1. Gold Ore
  2. Copper Ore
  3. Nickel Ore
  4. Other Base Metals (Lead, Zinc, etc.)
  5. Uranium Ore
  6. Vanadium Ore
  7. Iron Ore
  8. Mineral Sands
  9. Bauxite
  10. Miscellaneous Test

Gold Ore

Head Assay:

  • Gold: to check the valuable metal level.
  • Sulphur: to check the oxidation degree of the mineralisation.
  • Other metals: by Inductively Coupled Plasma (ICP) scan to perform a wide spread check for other metals, both beneficial and deleterious.
  • Arsenic content.
goldmineralogy

Gold mineralogy:

  • Pyrite
  • Pyrrhotite
  • Magnetite
  • Chalcopyrite
  • Bismuth
  • Bismuthinite
  • Galena

 

 

 

True Specific Gravity

The true specific gravity is determined on ground sample to remove the affect of sample porosity. Determination of true specific gravity of the ore is required for design and is used in any process calculations.


Comminution Testwork:

Comminution is the use of crushing and grinding to effect a reduction in particle size of the ore to liberate the valuable minerals from the gangue.

  • JK Drop Weight Test (DWT)
  • SAG Mill Comminution Test (SMC)
  • Point Load Test (PLT)
  • Unconfined Compressive Strength (UCS)
  • Abrasion Index (AI)
  • Crushing Work Index (CWI)
  • Bond Rod Mill Work Index (RWI)
  • Bond Ball Mill Work Index (BWI) 
Grind Establishment:

The grind establishment test is used to determine the relationship between the laboratory mill, grind time and resulting grind size. The samples will be ground for various times in the laboratory grinding mill and size analyses will be conducted on the grind products.

GrindDiagnostic Leach Test:

To check the distributions of gold in the samples. A diagnostic leach is a sequence of leaches using different solvents to differentiate the various gold associations.


Gravity Separation Test (Knelson or Falcon Test):

A portion of the composite will be subjected to gravity separation prior to conventional leaching. The removal of free gold, in particular, and silver, if present in economical quantities, prior to the traditional leaching processes has a number of advantages. Notably:

  • Decrease the circulating load of precious metals in the grinding circuit.
  • Potentially significant increase in overall recovery as particles of metallic gold are captured and treated, reducing the possibility of gold escaping as incompletely leached grains through the tails.
  • Carbon requirements are lower in the major leaching process.

Gravity Separation Test

Intensive Cyanide Leach (LeachWELL) Test:

Determines the recovery and gold production by leaching the concentrate (from Gravity Separation) using an ACACIA type reactor.  This test allows a more accurate assessment of the gravity concentrate as this product contains coarse, free gold which is very hard to assay. The size of the Intensive Leach Reactor is determined from the leach rates and the required throughput. Laboratory tests have proven to be very reliable in predicting full scale performance.

Intensive Cyanide Leach

 

 

Cyanide Leach Grind Sensitivity Test:

Determines the most economic grind size for leaching.  This will be the size that gives the best compromise between grinding costs and precious metal recovery.

Cyanide Leach Concentration Test:

Determines the optimum cyanide concentration at the optimum grind size for best gold recovery.

Oxygen Uptake Test:

Indicates the presence of any impurities which will consume oxygen and hence affect the leach kinetics.  It will indicate the possible need for air or oxygen addition during leaching.

Optimised Agitation Leach Test:

Utilises the optimum conditions of grind size, cyanide concentration and oxygen level to determine the overall amenability of the ore to agitated leaching.

Tailings Settling Test:

Evaluates the type of flocculant and the dosage required for any tails thickener. The results can also be used to provide a preliminary sizing of the thickener.

Lead Nitrate Test:

Evaluates whether lead nitrate enhances the leach test.  The presence of lead in the leach circuit is known to improve leach kinetics in some ores.

CIP Cyclic Carbon Loading Test:

Determines the suitability of carbon adsorption in the CIP technique for extraction of the gold.

Detox Test:

Detoxification tests are performed on leach tailings to examine the response of the ore to a detox method. There are a number of free cyanide destruction methods, including the INCO process. This process involves adding copper sulphate solution to the slurry (to complex the residual free cyanide) and then oxidising the cyanide with sulphur dioxide and air.  Detoxification of tailings solutions is of vital importance in ensuring that any operation meets environmental controls. It is of particular significance when the water balance within a plant is in surplus and hence water must be discharged.  The results from the detox test will give the conditions required for the INCO process to achieve acceptable cyanide and metal contents.

Cyanide Speciation:

Cyanide speciation tests determine what form the cyanide is present as in the tailings. The toxicity of cyanide is very dependent on the speciation of the cyanide present. Results from the test include total cyanide, weak acid dissociable cyanide and the whole range of metal cyanide complex speciation. This information is essential in the choice of appropriate cyanide removal or recovery technologies.

Beneficiation Tests:

Beneficiation in the minerals industry is the process of upgrading the average metal content of the process feed through the selective separation from a low grade component at some point in the comminution train. This can be done by a series of the screening, and scrubbing tests depending on the nature of the ore to determine if it is deemed to improve the gold and silver grade.

Crush Size Sensitivity Bottle Roll Test:

This test will provide information on the relationship between the crush size and the recovery possible. From this test the optimum crush size for heap leaching can be determined.

Crush Size Sensitivity Bottle Roll
Percolation Test:

The purpose of percolation tests is to determine the permeability of the ore to the leach solution at the optimum crush size. A percolation test will give a good idea of whether agglomeration will be required or not.

PercolationAgglomeration Test:

The agglomeration test establishes the optimum agglomerate size, binder amount and strength for optimum heap construct.

Column Leach Test:

The column leach test is a large scale heap leach test conducted over a 30 day period. This test is designed to properly gauge the extraction possible using heap leaching.

Column LeachSlurry Viscosity Test:

The viscosity of the slurry at a typical range of pulp density is determined.  If the viscosity is high then some correction factors need to be applied to the design or special equipment should be used in some sections of the plant.

Flotation Test:
This test assesses Gold, Silver and Sulphur recovery at various grind P80 (typically 75 microns, μm) and identifies flotation characteristics of the ore body. Froth flotation tests used to separate the refractory sulphides and precious metals from mineral gangue. The deportment of minerals to concentrate and tailings can be calculated for one stage of flotation. Scavenging and cleaning flotation processes can be assessed from the bulk rougher test. The concentrate from the bulk rougher float test will be assayed for its gold content. The tailings from the rougher float test will be assayed for gold content. The tailings will also be sized.

Flotation

 

Copper Ore

Head Assay :

Head assay is used to identify the more prospective elements and other elements that can be deleterious during extraction process of a copper ore. From the head assay, it is important to identify whether the copper is either sulfide or oxide in nature to determine the best processing route as the next step to extract the copper from the ore. Evaluating the amount of impurities such as Hg, As, Bi is also important as they can be problematic during the processes

Mineralogy :

  • Chalcopyrite
  • Bornite
  • Chalcocite
  • Covellite
  • Malachite
  • Cuprite
  • Tenorite
  • Tennanite
  • Tetrahydrite

Comminution : See gold ore section

True Specific Gravity : See gold ore section

Grind Establishment :See gold ore section

Size Assay :

The size analysis performed provides an idea of the amount of copper distributed at different size fractions.

Floation (Copper Sulphides):

The flotation process separates the different minerals into their respective fractions by using their different physical and chemical surface characteristics. The addition of chemical flotation reagents then causes the valued minerals to attach to air bubbles and rise to the surface of the tank where they overflow as a concentrate. Reagent dosage, kinetics, recovery and grades are studied.

Locked Cycle Floataion Test (Copper Sulphides) :

Usually, a locked cycle flotation test is done to:

  • To determine the increase in recovery obtained by recirculation cleaner tailing (or, to know the effect of recycling);
  • To determine the variation of reagent requirements to compensate for the circulation load of reagents;
  • To determine the effect of build-up of slimes that may interfere with the flotation;
  • To determine the froth flotation problems that may arise

The result can give the parameters used to design the flotation circuit, such as the number of roughers, scavengers, and cleaners required to achieve the target recovery and grade.

Column Flotation Test :

Instead of conventional cell used for flotation, column flotation test is sometimes needed. The objectives of the column flotation test are similar to the conventional flotation cell test. Another additional objective, for example, is to perform percolation test. Column flotation can be used for roughing, scavenging, and cleaning.

column floation

Thickening and Filtration Testwork :

Following flotation, the concentrate and tails products are thickened and filtered to assess the characteristics of the products at hand.The thickening tests will evaluate the thickening properties. The filtration results will help evaluate the filter performance and cycle time based on the laboratory conditions tested.

Thickening and Filtration

Heap Leach Amenability Testwork (Copper Oxides) :

Particularly useful when assessing the suitability of an ore for heap leaching. Leaching kinetics, metal recovery, acid consumption, slumping, percolation rate are variables that can be optimised in this testwork.

Direct Leaching :

Direct leaching is a term used to describe the leaching of all of an ore without prior beneficiation. This test can determine the optimum reagent concentration at the optimum grind size for best copper recovery by varying parameters such as grind size, reagent pH, etc.

Solvent Extraction :

This test provides an indication of the extraction and stripping kinetics as well as the phase separation behaviour for the extraction of copper from leached solution. Factors that are investigated during this test are:

  • Operating temperature
  • Viscosity of organic phase
  • Entrainment level
  • Copper in organic loading and extraction efficiency
  • Stage efficiencies, etc.
Solvent Extraction

Bacterial Leaching (Copper Sulfides) :

Bacterial leaching is suitable for copper sulfides as they oxidise the sulfur minerals to acquire energy to live, grow and reproduce. The bacteria produce sulfuric acid and copper sulfate. Recovery of the copper from the sulfate solution would be conducted in the later stages of the testwork. The testwork conducted for bacterial leaching would investigate key data such as kinetics, metal recovery and reagent consumption based on certain bacterium.

Pressure Oxidation (POX) Test :

This test is mainly used to determine metal recovery and evaluate and optimise operating conditions, such as pressure, temperature, monitor acid consumption and leach kinetics. Temperature is a critical variable as it influences the kinetic of leaching, and ultimately affects the residence time within the autoclave.

Variability Testwork: See gold ore section

 

Nickel Ore

Head Assay :

Head assay is used to identify the more prospective elements and other elements that can be problematic during extraction process of a nickel ore.

Mineralogy :

  • Sulphide
  • Oxide (Laterite)
  • Pentlandite
  • Pyrrhotite
  • Garnierite
  • Gersdorffite
  • Millerite
  • Niccolite
  • Breithauptite

Comminution : See gold ore section

Beneficiation Testwork (Nickel Oxides) :

Beneficiation Test is carried out to determine the nickel content of the ore at various different sizes. A number of size fractions are used to identify the Ni distribution and to determine if there is any barren Ni fraction, especially within the finer size. Such beneficiation result may indicate a certain size range needed for the Ni recovery. A series of wet and/or dry screening are used in beneficiation of an oxide nickel ore.

Bottle Roll Leach Text (Nickel Oxides) :

Bottle leach test is used to determine the maximum nickel recovery profile over time in a concentrated acid solution. Moreover, it is also used to determine maximum acid consumption.

Agglomeration Test :

Agglomeration is done by tumbling the ore with a binder to give the sample strength for supporting the mass of mineralisation. Agglomeration is done prior to the percolation test.

Percolation Test :

Percolation test is carried out to determine if the agglomerated fine grains have better percolation rate and lower slump than material with larger size fractions

Atmospheric and HPAL(High Pressure Acid Leach) Test :

HPAL Test is used for limonitic ores to determine Leach kinetics, nickel recovery, acid consumption of an ore.

POX (Pressure Oxidation) Test:

This test is mainly used to determine mineral recovery and design operating conditions, such as pressure, temperature, monitor acid consumption and leach kinetics. Temperature is a critical variable as it influences the kinetic of leaching, and ultimately affects the residence time within the autoclave

Heap Leach Amenability Testwork (Nickel Oxides):

This test is carried out to find if the ore is suitable for heap leaching. Leaching kinetics, metal recovery, acid consumption, slumping, percolation rate are variables that can be optimised in this testwork.

Oxygen Uptake Test : See gold ore section

Solvent Extration Testwork (Nickel Oxides) :

This test is performed in laboratory scale to determine the reagent dosage, operating pH, extraction, etc.

Batch Flotation Testwork (Nickel Sulphides) :

Batch flotation test is done to determine the most suitable collectors as well as the optimum concentration. The Flotation test results a set of data that is needed for designing the flotation circuit. Grind size, time recovery curve and grade recovery curve are the other data that can be obtained by carrying out this test.

Locked Cycle Floatation Test (Nickel Sulphides) :See Copper ore section

Variability Test:See gold ore section

 

Other Base Metals (Lead, Zinc, etc. )

Head Assay

Mineralogy

Comminution

Leach Test

Floataion Test

Thickening Test

Filtration Test

Uranium Ore

Head Assay

Mineralogy:

  • Uraninite
  • Pitchblende
  • Brannerite
  • Coffinite
  • Carnotite
  • Autunite
  • Davidite
  • Gummite
  • Torbernite
  • Uranophane

Comminution: See gold ore section

True Specific Gravity: See gold ore section

Grind Establishment: See gold ore section

Size Assay: See gold ore section

Floatation:

Thickening and Filtration Testwork

Heap Leach Amenability Testwork

Leaching

Solvent Extraction

Bacterial Leaching

Pressure Oxidation (POX) test

Variability Testwork: See gold ore section

 

Vanadium Ore

Head Assay

Mineralogy:

Magnetic Separation :

The vanadium ore may contain the magnetite/hematite mineral which is reduced to an appropriate size and passed over a series of low intensity; medium intensity (rare earth) and then high intensity magnetic separators.

This test aims to minimise the mass required to be finely milled and maximize the vanadium recovery. A sample of 20 kg of primary ore is to be evaluated at different grind size.

Roast Test:

The purpose of roast testwork is to obtain a flake product with a high vanadium recovery.

Leach Test

Precipitation Test

Variability Testwork: See gold ore section

 

Iron Ore

Head Assay

Mineralogy:

  • Magnetite
  • Hematite
  • Goethite
  • Siderite
  • Pyrite

Comminution : see gold ore section

Beneficiation Tests:

The Iron ore core sample is controlled crushed and subjected to Low Intensity Magnetic Separation (LIMS) or Rare Earth Magnetic Separation (REMS). Barren material (non-magnetic) separated from magnetic materials at coarse size will be rejected.The magnetic separation can be performed at different specified magnetic field intensities.

Other Metallurgical tests that can be carried out in the laboratories for iron ore beneficiation are:

  • Hydrosizer Simulation
  • Ultra Fine Grinding (Regrind)
  • Cleaning the Regrind Product
  • Davis Tube Test

Hydrosizer Simulation:

This test utilises mild centrifugal as well as gravitational forces to separate the valuable ore from the gangue material. An optional step, only performed should more gangue need to be removed from the magnetic concentrate prior to ultra fine grinding and magnetic separation.

Ultra Fine Grinding:

This technique is used to reduce particle size for increased silica liberation. To perform this test the magnetic separation concentrate will be subject to regrind at 38 µm, 28 µm and 20 µm prior to cleaning.

The regrind test work criteria may be revised based on the mineralogical survey.

Davis Tube Test :

This test determines separation characteristics of the ore under intensely controlled laboratory conditions on:

  • Sample of the regrind mill magnetic products
  • Reverse flotation magnetite concentrate

The test enables the efficiency of the cleaner separation processes to be compared.

The concentrate is reground to the optimum grind size to obtain concentrate grade. The yields and grade at various grinds are measured for the regrind samples and results related to cleaner testwork. Where possible, the standard industry test at 45µm should be performed on the ore, to ensure the consistency of the results.
Davis Tube

Magnetic Separation Test :

The principle of magnetic separation is to separate the magnetic iron ore, from the non magnetic gangue materials in order to produce. The basic factors needed for magnetic separator design are particle size range, magnetic characteristic of the feed, whether it is ferromagnetic, paramagnetic or diamagnetic, wet or dry processing, and desired throughput rate.

The proposed magnetic separation process is as follows:

Low Intensity Magnetic Separation (LIMS) at 800, 1000 and 1200 Gauss

Rare Earth Magnetic Separation (REMS)  at 3000, 4000 and 5000 Gauss
Wet High Intensity Magnetic Separation (WHIMS) at 8,000, 10,000 and 12,000 G
This aims to minimise the mass required to be finely milled and maximize the ore recovery. A sample of 100 kg of ore needs to be evaluated at three different sizes 300 µm, 212 µm and 150 µm prior to fine grinding.

Magnetic Separation

Flotation Test :

A 1 kg sample of the ore is ground to the required P80 particle size. The flotation test is conducted using the reagent scheme, conditioning times and froth removal times.

Each flotation product is filtered, dried and weighed before sub-samples are submitted for analysis.

This testwork is aimed at evaluating the characteristics of the final concentrate. These will include:

Concentrate Handling Testwork :

  • Thickening : Bench scale cylinder settling tests or vendor thickening tests are used to reduce final moisture content in the concentrate.
  • Filterability :Bench scale filter leaf tests or vendor filterability tests are used to measure the adaptability of a liquid-solid system to filtration
  • Blaine determination : This test is used to produce surface area measurement.

Tailings Tratment Testwork :

  • Thickening : Bench scale cylinder settling tests or vendor thickening tests are used to reduce final moisture content in the tailings.
  • Rheology : This tests evaluates the rheological properties (e.g. shear stress) of selected thickening samples, which could be used as a source for pipeline and pump design.

Mineral Sands

Head Assay

Mineralogy:

  • Ilmenite
  • Rutile
  • Leucoxene
  • Chromite
  • Tungsten
  • Magnetite
  • Zircon

Comminution Testwork

Magnetic Separation

Gravity Separation: Spiral

Electrostatic Separation:

This test is used to determine the non-conductors (zircon, monazite, quartz) and conductors (ilmenite, rutile) minerals in an ore.

Beneficiation

 

Bauxite

Head Assay

Mineralogy:

  • Gibbsite
  • Bohemite
  • Diaspore

Comminution Testwork

Digestion (Leach) Test

This test is used to determine the optimum temperature, caustic concentration and pressure for alumina extraction from bauxite ores.

Precipitation Test

Tailings Treatment Testwork :

  • Thickening
  • Filtering
  • Beneficiation Test

 

Miscellaneous Tests

Digestion (Leach) Test:

The principle of this test is using a liquid or suspension with density between minerals to be separated. All other gravity separations use a fluid less dense than the minerals. This test is used extensively to clean coal and for the concentration ore such as iron, lead-zinc, chrome, manganese, tin, tungsten, fluorspar, magnesite etc.

 


Variability Testwork


 

Variability test is used to find the suitability of the optimum process flowsheet across the ore body. This is also known as metallurgical mapping and tests the defined process by depth of sample or along strike and variability within domains.
A series of samples from various parts of the ore zones will be treated, at bench scale, using the optimised flowsheet, to test for consistency of the project ores’ responses to the treatment regime.
variability

Pilot Testing



Pilot testing is conducted:

  • to generate bulk concentrate and tailings samples for downstream process testwork (eg. roasting, thickening/settling, filtering);
  • to validate and optimise the bench scale flowsheet and provide additional information on operating parameters and potential problems;
  • to confirm the effect of flowsheet changes;
  • to confirm metallurgical response for continuous operation;
  • to increase confidence for capital raising, etc. and
  • to allow operator training prior to plant operation.
Pilot plant testing is generally seen as being more representative of plant processing than laboratory bench-scale tests. The successful pilot plant testing of an ore seems to evoke a sense of comfort with the flowsheet and reagent scheme. Pilot testing is a mandatory step for base metals ore.

There are several factors that can complicate this. The high cost involved in generating large quantities of sample for pilot plant testing can result in a compromised sample. Trial pits and shafts are usually mined to the minimum depth required. This can result in the inclusion of supergene or transitional material that may respond differently to the primary ore. Also, the sample is usually only from one specific area in the deposit which may differ significantly from the design ore type.
The cost of the sample generation can also result in short pilot runs. Pilot plants can be difficult to operate, and a lack of sample can result in less than optimum operating conditions due purely to time constraints. It is, therefore, crucial that pilot plant programs are carefully planned and managed.
Approximately 20-30 tonnes of ore sample are required to do pilot testing.

pilot

 

 


 
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